Electrochemical measurements of ascorbic acid based on graphite screen printed electrode modified with La3+/Co3O4 nanocubes transducer

Authors

  • Mohammad Reza Aflatoonian Research Center for Tropical and Infectious Diseases, Kerman University of Medical Sciences, Kerman amd Leishmaniasis Research Center, Kerman University of Medical Sciences, Kerman
  • Somayeh Tajik Research Center for Tropical and Infectious Diseases, Kerman University of Medical Sciences, Kerman
  • Behnaz Aflatoonian Neuroscience Research Center, Kerman University of Medical Sciences, Kerman
  • Hadi Beitollahi Environment Department, Institute of Science and High Technology and Environmental Sciences, Graduate University of Advanced Technology, Kerman

DOI:

https://doi.org/10.5599/jese.643

Keywords:

Ascorbic acid, electrochemical characterization, La3 /Co3O4 nanocubes, graphite screen printed electrode, voltammetry

Abstract

Electrochemical characterization of ascorbic acid oxidation on a graphite screen printed electrode (SPE) modified with La3+/Co3O4nanocubes is performed by applying cyclic voltammetry (CV), chronoamperometry (CHA), and differential pulse voltammetry (DPV) techniques. Synthesized La3+/Co3O4nanocubes for SPE modification, La3+/Co3O4/SPE, enhance the ascorbic acid electrooxidation kinetics by reducing the anodic overpotential. Excellent La3+/Co3O4/SPE electrochemical properties provide sensitive ascorbic acid voltammetric determination with low detection limit, good stability and quick response towards electrooxidation of ascorbic acid as compared to bare SPE. Under optimized conditions, DPV current demonstrates a linear response for ascorbic acid over a concentration range of 1.0 to 900.0 mM with a correlation coefficient of 0.9997, and detection limit (LOD) (S/N = 3) = 0.3 mM. The proposed procedure offers a potential application for producing the sensor with good repeatability. Also, fast response of fabricated sensor can allow a real-time analysis of real samples.

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Published

06-05-2019

How to Cite

Aflatoonian, M. R., Tajik, S., Aflatoonian, B., & Beitollahi, H. (2019). Electrochemical measurements of ascorbic acid based on graphite screen printed electrode modified with La3+/Co3O4 nanocubes transducer. Journal of Electrochemical Science and Engineering, 9(3), 197–206. https://doi.org/10.5599/jese.643

Issue

Section

Electrochemical Science

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