New modified mesoporous silica nanoparticles with bimetallic Ni-Zr for electroanalytical detection of dopamine

Original scientific paper

Authors

  • Mohamad Rafizie Aiman Mohamed Roduan Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia
  • Mohamad Idris Saidin Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia https://orcid.org/0000-0001-9735-7150
  • Siti Munirah Sidik Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia
  • Jaafar Abdullah Department of Chemistry, Faculty of Science, Universiti Putra Malaysia, 43400 Seri Kembangan, Selangor, Malaysia https://orcid.org/0000-0001-9686-4804
  • Illyas Md Isa Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia https://orcid.org/0000-0002-7621-2929
  • Norhayati Hashim Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia
  • Mohamad Syahrizal Ahmad Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia https://orcid.org/0000-0002-9278-6332
  • Siti Nur Akmar Mohd Yazid Department of Chemistry, Faculty of Science and Mathematics, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia https://orcid.org/0000-0002-9867-5641
  • Anwar Ul-Hamid Materials Characterization Laboratory, Centre for Engineering Research, Research Institute, King Fahd University of Petroleum and Minerals, Dhahran 31261, Saudi Arabia https://orcid.org/0000-0002-0259-301X
  • Aireen Aina Bahari Department of English Language and Literature, Faculty of Languages and Communication, Universiti Pendidikan Sultan Idris, 35900 Tanjong Malim, Perak, Malaysia https://orcid.org/0000-0003-2642-527X

DOI:

https://doi.org/10.5599/jese.1200

Keywords:

Porous material, nickel-zirconia, 3,4-Dihydroxyphenethylamine, electrochemical sensor, silica nanoparticles, modified GC electrode
Graphical Abstract

Abstract

In this research, bimetallic nickel-zirconia supported on mesoporous nanoparticles (Ni-Zr/MSN) were successfully synthesized by a simple in situ electrolysis method. Ni-Zr/MSN were well-characterized by Fourier transform infrared spectroscopy (FTIR), X-ray diffraction (XRD), X-ray photoelectron spectroscopy (XPS), Brunauer-Emmett-Teller (BET) analyzer, field emission scanning electron microscopy (FESEM), and transmission electron microscopy (TEM). Ni-Zr/MSN were then cast onto a modified glassy carbon electrode (Ni-Zr/MSN/GCE) as dopamine (DA) sensor. Under optimal conditions, the sensor showed a linear concen­tration relationship in the range of 0.3 µM–0.1 mM with a limit of detection of 0.13 µM. The relative standard deviation for 0.1 mM DA solution was 2.1 % (n = 5). The presence of excess catechol, saccharose, glycine, lactose, uric acid, and Cr3+, Fe2+ and Na+ as interferents was negligible, except for uric acid in 10-fold excess. The analytical recovery of the sensor was successfully demonstrated by the determination of DA in DA-containing medicine and wastewater samples. The results presented herein provide new perspectives on Ni-Zr/MSN as a potential nanomaterial in the development of DA sensors.

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Published

04-04-2022

How to Cite

Mohamed Roduan, M. R. A., Saidin, M. I., Sidik, S. M., Abdullah, J., Md Isa, I., Hashim, N., Ahmad, M. S., Mohd Yazid, S. N. A., Ul-Hamid, A., & Bahari, A. A. (2022). New modified mesoporous silica nanoparticles with bimetallic Ni-Zr for electroanalytical detection of dopamine: Original scientific paper. Journal of Electrochemical Science and Engineering, 12(3), 463–474. https://doi.org/10.5599/jese.1200

Issue

Vol. 12 No. 3 (2022)

Section

Electrochemical Science

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