Screen printed graphite electrode modified with two-dimen-sional leaf-like zeolitic imidazolate framework-L (Zn) for efficient electrochemical sensing of sulphite: Original scientific paper

Satar Jabbar Rahi Algraittee; Ban Waheed Hussein Bdair; Firas Abdul Abass Sukir; Raed Muslim Muhibes; Mustafa Mudhafar; Qais R. Lahhob

doi:10.5599/jese.2580

Authors

Satar Jabbar Rahi Algraittee College of Medicine, University of Kerbala, Kerbala, Iraq https://orcid.org/0000-0002-2124-3920
Ban Waheed Hussein Bdair Department of Medical Microbiology, College of Medicine, University of Kerbala, Kerbala, Iraq https://orcid.org/0000-0002-3313-0528
Firas Abdul Abass Sukir Department of Radiology, College of Health & Medical Technology, Sawa University, Iraq https://orcid.org/0009-0002-3676-9180
Raed Muslim Muhibes Department of Biochemistry, College of Medicine, Misan University, Misan, Iraq https://orcid.org/0000-0002-4835-0873
Mustafa Mudhafar Department of Medical Physics, Faculty of Medical Applied Sciences, University of Kerbala, 56001, Karbala, Iraq https://orcid.org/0000-0002-3785-7396
Qais R. Lahhob Collage of Pharmacy, National University of Science and Technology, Dhi Qar, 64001, Iraq https://orcid.org/0000-0001-5259-8946

DOI:

https://doi.org/10.5599/jese.2580

Keywords:

Differential pulse voltammetry, metal-organic frameworks, electrochemical sensors, chemically modified electrodes, real sample analysis

Abstract

In this paper, we describe the use of a screen-printed graphite electrode modified with a two-dimensional leaf-like zeolitic imidazolate framework-L (Zn), ZIF-L (Zn) for the deter¬mination of sulphite. We started by using linear sweep voltammetry to investigate the redox properties of the modified electrode at different scan rates (10 to 400 mV s^-1). Next, we evaluated sulphite oxidation in the modified electrode. Using differential pulse voltammetry (DPV), the linear dynamic range of 0.04-900.0 µM and the limit of detection (3s/m) of 0.01 μM were obtained. DPV was also used to quantify sulphite in various real samples using the standard addition method.

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Screen printed graphite electrode modified with two-dimen-sional leaf-like zeolitic imidazolate framework-L (Zn) for efficient electrochemical sensing of sulphite

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