Monitoring of nickel(II) in biological samples using 4-(2-hydroxy-phenylethamino)benzene-1,3-diol by extractive differential pulse polarography
DOI:
https://doi.org/10.5599/jese.318Keywords:
Monitoring, nickel(II), Extractive differential pulse polarographyAbstract
A novel analytical reagent, 4-(2-hydroxyphenylethamino)benzene-1,3-diol was synthesized for determination of nickel(II) in biological samples and plant materials by extractive differential pulse polarography. The analysis of nickel(II) was carried out by extracting the nickel(II)-(4-(2-hydroxyphenylethamino)benzene-1,3-diol) complex from chloroform prior to injecting into the instrument. The electrochemical behavior of nickel(II) complex was studied under optimum parameters like effect of pH, pulse amplitude, scan rate and choice of solvent. The calibration curve was constructed in the concentration range of 0.05-42 µg mL-1 at pH 4.0 (acetate buffer) with a correlation coefficient of 0.992, respectively. Interference of diverse ions was also investigated during the analysis of nickel(II) to optimize the conditions. The accuracy and validity of the proposed method were checked by the analysis of Certified Reference Materials which is distributed by the National Institute of Standard Technology
Downloads
References
J. J. Scott-Fordsmand, P. H. Krogh, S. P. Hopkin, Ecotox. Environ. Safe. 43(1) (1999) 57-61.
K. S. Kasprzak Mutat. Res. 533(1-2) (2003) 67-97.
E. Y. Hashem, M. S. Abu-Bakr, S. M. Hussain, Spectrochem. Acta A 59 (2003) 761-769.
Y. Liu, X. Chang. S. Wang.Y. Guo, B. Din, S. Meng, Talanta 64 (1) (2004)160-166.
Z. Augustynski, B. Dziunikowski, J. Meitin, J. Radioanal. Nucl. Chem. 63 (2) (1981) 325-334.J. L. Manzoori, A. Bavili-Tabrizi, Microchim. Acta 141(3-4) (2003) 201-207.
E. Vereda Alonso, A. Garcia de Torres, J. M. Cano Pavon, Mikrochim. Acta 110(1-3) (1993) 41-45.
S. L. C. Ferreira, C. F. de Brito, A. F. Dantas. N. M. Lopo de Araujo, A. C. S. Costa, Talanta 48(5) (1999) 1173-1177.
C. J. Park, S. A. Yim, J. Anal. Atom. Spectrom. 14 (1999) 1061-1065.
M. Korolczuk, Talanta, 53(3) (2000) 679-686.
N. Y. Sreedhar, D. Rekhs, Anal. Chem. Ind. J. 8(2) (2009) 209-212.
X. Yang. Z. Qiao. W. Wei, S. Yao, Talanta 46(4) (1998) 697-702.
C. J . Flora, E. Nieboer. Anal. Chem. 52(7) (1980) 1013-1020.
L. Larai, Y. Harek, A. Reguig, M. M. Mostafa, J. Serb. Chem. Soc. 68(2) (2003) 85-95.
W. P. Griffith, S. I. Mostafa, Polyhedron 11(23) (1992) 2997-3005.
T. Priya Devi, R. K. Hemakumar Singh, Rasayan Journal of Chemistry 3(2) (2010) 266-270.
D. Rekha, N. Y. Sreedhar, P. Reddy Prasad, Global Journal of Science Frontier Research 10(2) (2010) 21-29.
A. A. Almeida. X. Jun, J. L. F. C. Lima, Talanta 50(2) (1999) 253-259.
A. Praveen Kumar, P. Raveendra Reddy, V. Krishna Reddy, J. Autom. Method. Manag. 1 (2007) 1-6.
C. S. Kira, A. M. Sakuma, N. da Cruz Gouveia, Journal of Applied Pharmaceutical Science, 4(5) (2014) 39-45.
Z. Sun, P. Liang, Q. Ding, J. Cao, Hazard. Mater. B, 137(2) (2006) 943-946.
R. Galbeiro, S. Garcia, I. Gaubeur, J. Trace. Elem. Med. Bio. 28(2), (2014) 160-165.
Q. Hu, G. Yang, Z. Huang, J. Yin. Anal. Sci. 19(10) (2003) 1449-1452.
B. Saritha, T.S. Reddy, IOSR J. Appl. Chem. 7(3) (2014) 22-26.
H. Cyftci. A. Olcucu, T. Cyftci, International Journal of Science and Technology 2(2) (2007) 105-108.
Q. Hu, G. Yang, Z. Huang, J. Yin, B. Kor. Chem. Soc. 25(4) (2004) 545-548.
Downloads
Published
Issue
Section
License
Copyright (c) 2017 Journal of Electrochemical Science and Engineering
This work is licensed under a Creative Commons Attribution 4.0 International License.
